Page 9 - Synthesis of Functional Nanoparticles Using an Atmospheric Pressure Microplasma Process - LiangLiang Lin

3.
2.1 Multiphase Operational Microplasma Setup ..............................................................24
2.1.1 Initial Concept of the Microplasma Setup for the Gas-phase Nanofabrication ................ 24 2.1.2 Advanced Concept of the Microplasma Setup for the Gas-phase Nanofabrication .......... 25 2.1.3 Microplasma Setup for the Liquid-phase Nanofabrication ............................................... 26
2.2 Characterization Methodologies and Instrumentation Techniques ............................28
2.2.1 In-situ Characterization of the Plasma-assisted Precursors Dissociation Process .......... 28 2.2.2 Ex-situ Characterization of the Generated Nanoparticles ................................................ 29
2.3 Critical Safety Considerations....................................................................................36 References ........................................................................................................................37 Supplementary Material ...................................................................................................38
Iron Oxide Nanoparticles Synthesis and Mechanism Study - a Proof-of-Concept Model Study ................................................................................................................41
3.1 Introduction ................................................................................................................42
3.2 Experiment Section ....................................................................................................43
3.2.1 Experimental ...................................................................................................................... 43 3.2.2 Characterization ................................................................................................................ 43
3.3 Results and Discussion ...............................................................................................44
Table of Contents
1. Introduction - Plasma and Microplasma-assisted Nanofabrication ......................1
1.1 Conventional Nanomaterials Synthesis........................................................................2 1.2 Plasma-assisted Nanomaterials Synthesis ....................................................................3 1.3 Microplasma-assisted Nanomaterials Synthesis...........................................................5
1.3.1 Microplasma ........................................................................................................................ 5 1.3.2 Existing Microplasma Systems for Nanomaterials Synthesis .............................................. 7 1.3.3 Typical Applications of Nanoparticles............................................................................... 14
1.4 Research Aim and Scope............................................................................................18 References ........................................................................................................................19
2. Multiphase Operational Microplasma Setup and the Involved Instrumentation Techniques.................................................................................................................23